Direct Determination of Tin in Urine by Zeeman Atomic Absorption Spectrometry
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چکیده
منابع مشابه
Direct determination of zinc in serum by Zeeman atomic absorption spectrometry with a graphite furnace.
We developed a precise and accurate graphite furnace atomic absorption spectrometric method for the direct determination of zinc in serum. Serum samples are analyzed after 20-fold dilution with water of ultrapure analytical grade. No other reagent is used, from the moment of sampling until measurement. During atomization, the argon flow is kept at 150 mL/min instead of gas stop, to decrease the...
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The problems encountered in platform AAS determinations of selenium in biological fluids were recently reported by Carnrick et al. [1]. The presence of phosphates produces a spectral interference for the selenium determination at 196.0 nm, avoided by using Zeeman background correction. On the other hand, Hoenig and Van Hoeyweghen show that spectral interference of phosphates in animal tissues m...
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To study the possible accumulation of Sr in chronic renal failure patients, methods were developed for the determination of the element in serum, urine, bone, and soft tissues by using Zeeman atomic absorption spectrometry. Serum samples were diluted 1:4 with a Triton X-100-HNO3 mixture, whereas urine samples were diluted 1:20 with HNO3. Bone samples were digested with concentrated HNO3 in stop...
متن کاملImproved determination of selenium in serum by Zeeman atomic absorption spectrometry.
We have improved Zeeman atomic absorption spectrometric determination of selenium in serum by using an acidic solution of Ag + Cu + Mg as a matrix modifier and performing the charring step in flowing O2. Under these conditions, we could calibrate serum results with selenium standards in bovine albumin solutions. Mean analytical recovery was 98%, and the CV was 1.8% within runs, 2.9% between run...
متن کاملDetermination of Aluminum in Dialysis Concentrates by Atomic Absorption Spectrometry after Coprecipitation with Lanthanum Phosphate
This method was developed for the determination of trace amounts of aluminum(III) in dialysis concentrates using atomic absorption spectrometry after coprecipitation with lanthanum phosfate. The analytical parameters that influenced the quantitave coprecipitation of analyte including amount of lanthanum, amount of phosfate, pH and duration time were optimized. The % recoveries of the analyte io...
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ژورنال
عنوان ژورنال: Sangyo Igaku
سال: 1983
ISSN: 0047-1879,1881-1302
DOI: 10.1539/joh1959.25.7_701_3